1) Benzene, 1-bromo-2-chloro-
邻氯溴苯
2) 1-Bromo-2-chlorobenzene
邻氯溴苯
3) o-Bromochlorbenzene
邻氯溴苯
4) o-chlorophenol
邻氯酚
1.
Study on microwave-assisted regeneration of hypercrosslinked polymeric adsorbent adsorbing o-chlorophenol;
吸附邻氯酚的超高交联树脂微波辅助再生研究
2.
Sorption properties of phenol,o-chlorophenol,2,4-dichlorophenol on four kinds of suspended particles sampled from Changjiang Estuary and Hangzhou Bay were investigated.
研究了4种分别取自长江口和杭州湾的悬浮泥沙样品对苯酚、邻氯酚和2,4-二氯酚的吸附特性。
5) o-chlorobenzyl chloride
邻氯氯苄
1.
The preparation of o-chlorobenzaldehyde from the residual liquid generated in the production of o-chlorobenzyl chloride;
由生产邻氯氯苄的残液制备邻氯苯甲醛
2.
According to the main problem of current synthesis of o-chlorobenzyl chloride in our country,effective improvement was studied to increase the reaction conversion to 60% by use of a new catalyst CHJ-3.
针对目前国内邻氯氯苄生产工艺存在的主要问题,通过选用新型催化剂CHJ-3,改进催化氯化工艺,使氯化反应邻氯甲苯转化率达到60%。
3.
Taking o-cholorotoluene as raw material,the factors influencing the photochlorination synthesis of the o-chlorobenzyl chloride were investigated.
研究了邻氯甲苯光氯化生成邻氯氯苄的各项影响因素,在适宜条件下,邻氯甲苯的转化率可达75%以上,反应过程邻氯氯苄的收率可达90%。
6) o-chloroaniline
邻氯苯胺
1.
MOCA is prepared with o-chloroaniline and paraformaldehyde as materials.
以邻氯苯胺和多聚甲醛为反应原料制备MOCA。
2.
The cheap available starting material,O-chloroaniline,reacted with trichloroacetaldehyde monohydrate and hydroxylamine hydrochloride to produe N-(2-chlorophenyl)-2-(hydroxyimino) acetamide;which was treated with concentrated sulfuric acid to obtained 3-chlorolisatin,then 3-chlorolisatin was oxidized by hydrogen peroxide to afford 2-amino-3-chlorobenzoic acid.
以邻氯苯胺为原料,与水合三氯乙醛、盐酸羟胺反应先制得邻氯基(N-肟基乙酰)苯胺,用浓硫酸关环生成3-氯靛红。
3.
A series of titania-supported nickel catalysts with different Ni loadings (10%~40%) were prepared by the incipient impregnation method and applied in the hydrogenation of o-chloronitrobenzene to o-chloroaniline.
用等体积浸渍法制备了一系列不同镍负载量的负载型Ni/TiO2催化剂,并将其应用于邻氯硝基苯加氢制邻氯苯胺的反应。
参考词条
补充资料:邻氯溴苯
分子式:C6H4BrHCl
分子量:191.45
CAS号:694-80-4
性质:无色液体。熔点-12.3℃,沸点204℃(195℃),闪点79℃,相对密度1.6378(25/4℃),折光率1.5809,闪点79℃。能溶于苯,不溶于水。
制备方法:由邻氯苯胺重氮化,再与溴化亚铜反应而得。将邻氯苯胺与48%的氢溴酸混合,加冰降温到0℃,于搅拌下迅速加入亚硝酸钠水溶液,加碎冰使温度保持在10℃以下。然后将氯化亚铜和氢溴酸混合物加热至沸后加入重氮液。控制重氮液加入速度,维持反应在沸腾下进行。重氮液加完后,产物随水蒸气蒸出,从馏出液中分离出有机相(下层液),用浓硫酸洗涤,水洗,用5%氢氧化钠溶液洗,再用氯化钙干燥后蒸馏,收集199-201℃(98.4kPa)馏分即为成品。
用途:有机合成中间体,溶剂。
分子量:191.45
CAS号:694-80-4
性质:无色液体。熔点-12.3℃,沸点204℃(195℃),闪点79℃,相对密度1.6378(25/4℃),折光率1.5809,闪点79℃。能溶于苯,不溶于水。
制备方法:由邻氯苯胺重氮化,再与溴化亚铜反应而得。将邻氯苯胺与48%的氢溴酸混合,加冰降温到0℃,于搅拌下迅速加入亚硝酸钠水溶液,加碎冰使温度保持在10℃以下。然后将氯化亚铜和氢溴酸混合物加热至沸后加入重氮液。控制重氮液加入速度,维持反应在沸腾下进行。重氮液加完后,产物随水蒸气蒸出,从馏出液中分离出有机相(下层液),用浓硫酸洗涤,水洗,用5%氢氧化钠溶液洗,再用氯化钙干燥后蒸馏,收集199-201℃(98.4kPa)馏分即为成品。
用途:有机合成中间体,溶剂。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。