1) o-Chlorobenzonitrile
邻氯苯腈
2) 2-Chlorobenzonitrile
邻氯苯腈
3) 2 chlorobenzonitrile
邻氯苯腈
1.
o Flurobenzonitrile(OFBN) was prepared from 2 chlorobenzonitrile and KF using sulfolane as a solvent.
以邻氯苯腈 (OCBN)和氟化钾为原料 ,环丁砜为反应介质 ,经氟化反应合成了邻氟苯腈。
4) o-chlorophenol
邻氯酚
1.
Study on microwave-assisted regeneration of hypercrosslinked polymeric adsorbent adsorbing o-chlorophenol;
吸附邻氯酚的超高交联树脂微波辅助再生研究
2.
Sorption properties of phenol,o-chlorophenol,2,4-dichlorophenol on four kinds of suspended particles sampled from Changjiang Estuary and Hangzhou Bay were investigated.
研究了4种分别取自长江口和杭州湾的悬浮泥沙样品对苯酚、邻氯酚和2,4-二氯酚的吸附特性。
5) o-chlorobenzyl chloride
邻氯氯苄
1.
The preparation of o-chlorobenzaldehyde from the residual liquid generated in the production of o-chlorobenzyl chloride;
由生产邻氯氯苄的残液制备邻氯苯甲醛
2.
According to the main problem of current synthesis of o-chlorobenzyl chloride in our country,effective improvement was studied to increase the reaction conversion to 60% by use of a new catalyst CHJ-3.
针对目前国内邻氯氯苄生产工艺存在的主要问题,通过选用新型催化剂CHJ-3,改进催化氯化工艺,使氯化反应邻氯甲苯转化率达到60%。
3.
Taking o-cholorotoluene as raw material,the factors influencing the photochlorination synthesis of the o-chlorobenzyl chloride were investigated.
研究了邻氯甲苯光氯化生成邻氯氯苄的各项影响因素,在适宜条件下,邻氯甲苯的转化率可达75%以上,反应过程邻氯氯苄的收率可达90%。
6) o-chloroaniline
邻氯苯胺
1.
MOCA is prepared with o-chloroaniline and paraformaldehyde as materials.
以邻氯苯胺和多聚甲醛为反应原料制备MOCA。
2.
The cheap available starting material,O-chloroaniline,reacted with trichloroacetaldehyde monohydrate and hydroxylamine hydrochloride to produe N-(2-chlorophenyl)-2-(hydroxyimino) acetamide;which was treated with concentrated sulfuric acid to obtained 3-chlorolisatin,then 3-chlorolisatin was oxidized by hydrogen peroxide to afford 2-amino-3-chlorobenzoic acid.
以邻氯苯胺为原料,与水合三氯乙醛、盐酸羟胺反应先制得邻氯基(N-肟基乙酰)苯胺,用浓硫酸关环生成3-氯靛红。
3.
A series of titania-supported nickel catalysts with different Ni loadings (10%~40%) were prepared by the incipient impregnation method and applied in the hydrogenation of o-chloronitrobenzene to o-chloroaniline.
用等体积浸渍法制备了一系列不同镍负载量的负载型Ni/TiO2催化剂,并将其应用于邻氯硝基苯加氢制邻氯苯胺的反应。
参考词条
补充资料:邻氯苯腈
分子式:C7H4ClN
分子量:137.57
CAS号:873-32-5
性质:针状结晶。熔点43-46℃,沸点232℃,闪点108℃。溶于乙醚、乙醇。
制备方法:由邻氯苯甲酸与尿素反应而得:将邻氯苯甲酸、氨基磺酸和尿素混合后加热至140℃左右熔融,在搅拌下剧烈反应,并放出大量气体,温度自动上升至220-230℃,反应2h。然后冷却至15℃以下,过滤,所得固体分别用3%氨水和水洗至中性,再经干燥而得成品。
用途:有机合成中间体。主要用于合成染料中间体2-氰基-4-硝基苯胺,医药工业用于合成抗疟疾新药硝喹等。
分子量:137.57
CAS号:873-32-5
性质:针状结晶。熔点43-46℃,沸点232℃,闪点108℃。溶于乙醚、乙醇。
制备方法:由邻氯苯甲酸与尿素反应而得:将邻氯苯甲酸、氨基磺酸和尿素混合后加热至140℃左右熔融,在搅拌下剧烈反应,并放出大量气体,温度自动上升至220-230℃,反应2h。然后冷却至15℃以下,过滤,所得固体分别用3%氨水和水洗至中性,再经干燥而得成品。
用途:有机合成中间体。主要用于合成染料中间体2-氰基-4-硝基苯胺,医药工业用于合成抗疟疾新药硝喹等。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。