1) 2-Aminodiphenyl
邻苯基苯胺
2) o-nitro-aniline
邻硝基苯胺
1.
The synthetic process of 2-acetyl-3-methylquinoxaline-1,4-dioxide was studied,which was synthesized in over all yield of 86% by the oxidation of o-nitro-aniline and Beirut reaction of benzofuraxan and acetylacetone.
以邻硝基苯胺为起始原料,经过氧化反应和Beirut反应,以86%的总收率制得产物2-乙酰基-3-甲基喹噁啉-1,4-二氧化物。
3) o-toluidine
邻甲基苯胺
1.
The resolution was 4 for the separation of the most difficult isomers such as o-toluidine and p-toluidine.
该柱对邻甲基苯胺、间甲基苯胺、对甲基苯胺同分异构体显示了很好的色谱分析性能。
2.
Indole has been prepared by the reaction of O-toluidine and formic acid to obtain N-formacyl-O-toluidine(O-toluidide),then in the presence of potassium hydroxide by toluone and O-toluidine used as water carrying reagent and solvent converted furter into potassium salt of O-toluidide,followed cyclization and hydrolysis.
用邻甲基苯胺和甲酸反应制得N-甲酰基邻甲基苯胺(甲酰化物),然后在氢氧化钾存在下,用甲苯作带水剂,邻甲基苯胺作溶剂制得甲酰化物钾盐,接着环合、水解制得吲哚,其收率达65%。
3.
Synthesize saframine O using o-toluidine as primer reactant by diazotization, coupling reaction, reduction reaction, and oxidation.
研究了以邻甲基苯胺为起始原料,经重氮化、偶合、还原、氧化反应合成藏花红的方法。
4) o-nitroaniline
邻硝基苯胺
1.
In the presence of urushibara nickel catalyst, o-phenylenediamine was prepared by catalytic hydrogenation of o-nitroaniline at ambient pressure and 45℃.
以漆原镍(U Ni A)作催化剂,在45℃常压下将邻硝基苯胺氢化还原为邻苯二胺,加氢转化率达98%,催化剂能重复回收套用10次。
2.
In this paper,the one-pot reaction of aqueous titanium trichloride with o-nitroaniline and 1,2-diketone compounds in basic media was studied.
研究三氯化钛存在下邻硝基苯胺与1,2-二酮在碱性介质中一锅反应,快速方便、高收率地合成了一系列取代喹喔啉化合物。
3.
Using o-nitroaniline as the starting material, benzimidazoles were prepared by the way of one-pot synthesis in the system of SnCl2·2H2O/KI/HCl at the temperature of 100 ℃.
以邻硝基苯胺为原料,在SnCl2·2H2O/KI/HCl体系中,100℃条件下,一锅法合成12种苯并咪唑化合物。
5) O-aminophenol
邻胺基苯酚
1.
Cooperative effect of inhibiting H2 evolution for stannate and O-aminophenol on Al anode;
锡酸钠与邻胺基苯酚对铝阳极的共同抑氢作用
2.
The effect of inhibiting H_2-evolution for O-aminophenol on Al-alloy anode in 4 mol/L KOH was studied by galvanostatic gathering volumes of hydrogen evolution and stable state polarization curves and electrochemical impedance spectrum.
通过恒电流集气、稳态极化曲线、交流阻抗等电化学方法探讨了邻胺基苯酚在4 mol/L KOH溶液中对Al-0。
补充资料:邻苯基苯胺
分子式:C12H11N
分子量:169.23
CAS号:90-41-5
性质:无色或微紫色结晶。熔点49-50℃,沸点299℃,170℃(2.0kPa),145-148℃(0.67kPa)。溶于醇、醚和苯,不溶于水。能随水蒸气挥发。闪点>110℃。
制备方法:以邻硝基联苯为原料,经还原而得:将邻硝基联苯、乙醇、氯化亚锡于水浴回流3h,回收乙醇,将剩余物冷却,加入40%液碱使呈强碱性,分出油层,水层用乙醚提取,将提取液用无水氯化钙干燥,过滤回收乙醚,用乙醇洗得粗品,再将粗品减压蒸馏而得成品。
用途:用作有机合成的原料。制造咔唑树脂,合成橡胶。
分子量:169.23
CAS号:90-41-5
性质:无色或微紫色结晶。熔点49-50℃,沸点299℃,170℃(2.0kPa),145-148℃(0.67kPa)。溶于醇、醚和苯,不溶于水。能随水蒸气挥发。闪点>110℃。
制备方法:以邻硝基联苯为原料,经还原而得:将邻硝基联苯、乙醇、氯化亚锡于水浴回流3h,回收乙醇,将剩余物冷却,加入40%液碱使呈强碱性,分出油层,水层用乙醚提取,将提取液用无水氯化钙干燥,过滤回收乙醚,用乙醇洗得粗品,再将粗品减压蒸馏而得成品。
用途:用作有机合成的原料。制造咔唑树脂,合成橡胶。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。
参考词条