1) chlorosulfonation
氯磺酰化
1.
B15C5 was readily converted to the highly pure 4′ chlorosulfonylbenzo 15 crown 5(2) by chlorosulfonation with chlorosulfonic acid at ambient temperature,then reduction of the sulfonyl chloride moiety in 2 with zinc and sulfuric acid provided the 4′ mercaptobenzo 15 crown 5 in good yield.
在室温下用氯磺酸将苯并-15-冠-5 氯磺酰化,制备高纯度的4′-氯磺酰基苯并-15-冠-5,然后用Zn/硫酸将氯磺酰基还原,制得较高产率的 4′-巯基苯并-15-冠-5。
2) chlorosulfonylation,chlorosulfonation
氯磺(酰)化
3) chlorosulfonation
氯磺化
1.
Synthesize 2-methyl-5-acetamino benzene sulfochloride using p-toluidine as primer reactant by aceylation and chlorosulfonation.
以对甲基苯胺为起始原料,通过乙酰化和氯磺化反应合成2-甲基-5-乙酰氨基苯磺酰氯(Ⅰ)。
2.
During the chlorosulfonation of N-acetanilide to p-acetamidobenzenesulfonyl chloride,sodium sulphate was added in late stage.
改进后,氯磺化的收率明显提高,废弃物排放量减小。
3.
In the reaction of chlorosulfonation carbon tetrachloride was used as solvent,adding the sodium chloride in later stage reaction.
以苯胺为母体合成对乙酰氨基苯磺酰胺,在氯磺化反应中引入四氯化碳作溶剂,在反应后期加入氯化钠。
4) sulfochlorination
氯磺化
1.
To improve the synthetic technology,albendazole is synthesized from carbendazole by sulfochlorination,reduction of iron powder and thiolation under alkalinious catalyst condition.
以价廉易得的农药多菌灵为原料,经氯磺化、铁粉还原、碱催化条件下硫醚化合成了阿苯达唑,并对氯磺化、还原和硫醚化工艺进行改进。
2.
2,4-Dichloro-5-sulfamoylbenzoic acid(1)was synthesized by sulfochlorination, ammoniation and hydrolysis with 2,4-dichlorobenzoic acid as raw materials, and the reaction conditions were optimized.
2,4-二氯苯甲酸为原料,经氯磺化、氨解、水解酸化三步反应制备了2,4-二氯-5-磺酰氨基苯甲酸(1)。
5) chlorsulfuron
氯磺隆
1.
Screening,Immobilization and Characters Studying on the Superior Mic roorganisms Strains for Degradation of Chlorsulfuron;
氯磺隆降解优势菌的筛选固定化及特性研究
2.
Studies on the herbicide safener 3-dichloracetyl-2,5-dimethyl-2-ethyl-1,3-oxazolidine for reducing injury by chlorsulfuron to corn;
3-二氯乙酰基-2,5-二甲基-2-乙基-1,3-噁唑烷减轻氯磺隆对玉米的伤害作用研究
3.
Study on Enzymatic Inhibition of Acetolactate Synthase from Maize (Zea mays L. ) by Chlorsulfuron and Tribenuron-methyl;
氯磺隆和苯磺隆对玉米乙酰乳酸合成酶抑制作用的研究
6) Chlorosulfophenol K
氯磺酚K
1.
Study on the Interaction of Serum Proteins with Chlorosulfophenol K and Its Analytical Application;
血清蛋白质与氯磺酚K反应及其分析应用的研究
参考词条
补充资料:氯次磺酰化
分子式:
CAS号:
性质:在有机化合物分子中引入氯次磺酰基(-SCl)而生成次磺酰氯的反应。次磺酰氯是由二硫化物经氯解生成的,例如:[CH3(CH2)4S]2+Cl2→CH3(CH2)4SCl次磺酰氯可用做氨基保护基试剂。
CAS号:
性质:在有机化合物分子中引入氯次磺酰基(-SCl)而生成次磺酰氯的反应。次磺酰氯是由二硫化物经氯解生成的,例如:[CH3(CH2)4S]2+Cl2→CH3(CH2)4SCl次磺酰氯可用做氨基保护基试剂。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。