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1)  ethoxynaphthoquinone
乙氧基萘醌
2)  azo-compounds
萘氧基萘并萘醌
3)  phenoxynaphthacenequinone
苯氧基萘并萘醌
1.
A new photochromic phenoxynaphthacenequinone polymer with ethylene-maleic anhydride copolymer as main chain (4) was synthesized at first by the reaction of 3-bromopropan-1-ol (1) with 6-henyl)isopropyl)phenoxy]-5,12-naphthacenequinone (2) to prepare a new reagent, 6- -5,12-naphthacenequinone (3), and then by the reaction of (3) with an ethylene-maleic anhydride alternative copolymer.
通过由3-溴丙-1-醇(1)与6-[4-(2-(4-羟基苯基)异丙基)苯氧基]-5,12-萘并萘醌(2)反应制备新反应试剂6-[4-(2-(4-(3-羟基丙氧基)苯基)异丙基)苯氧基]-5,12-萘并萘醌(3),然后通过(3)与乙烯-顺丁烯二酸酐交替共聚物反应的方法成功合成了乙烯-顺丁烯二酸酐为主链的光致变色苯氧基萘并萘醌聚合物(4)。
2.
Three dichromogenic compounds containing both phenoxynaphthacenequinone and azobenzene photochromes, 6 [4 (phenylazo)phenoxy] 5,12 naphthacenequinone(5), 6 [4 ( p ethoxyphenylazo)phenoxy] 5,12 naphthacenequinone(6) and 6 [4 ( p nitrophenylazo)phenoxy] 5,12 naphthacene quinone(7), were synthesized by reacting 6 chloro 5,12 naphthacene quinone with 4 hydroxyazobenzene and its derivatives.
通过6-氯-5,12-萘并萘醌与4-羟基偶氮苯及其衍生物的反应合成了3种含苯氧基萘并萘醌和偶氮苯光致变色基的双变色基化合物,6-[4-(苯偶氮基)苯氧基]-5,12-萘并萘醌(5),6-[4-(p-乙氧基苯偶氮基)苯氧基]-5,12-萘并萘醌(6)和6-[4-(p-硝基苯偶氮基)苯氧基]-5,12-萘并萘醌(7)。
3.
9-hydroxy-10-phenoxy-l, 4-anthraquinone and phenol aldehyde resin containing photochromic phenoxynaphthacenequinone have been synthesized and characterized by H-NMR, IR and UV-VIS spectroscopy.
本文在综述国内外文献的基础上,选取苯氧基醌类光致变色材料为研究对象,尝试了苯氧基蒽醌类、苯氧基萘并萘醌类化合物及聚合物的合成。
4)  2-(Acetyloxy)-3-dodecyl-1,4-naphthalenedione
2-(乙酰氧基)3-十二烷基-1,4-萘醌
5)  β-naphthyl ethyl ether
2-乙氧基萘
6)  Ethyl 1-naphthyl ether
1-乙氧基萘
补充资料:1-乙氧基萘
分子式:C12H12O
分子量:172.23
CAS号:5328-01-8

性质:无色油状液体或针状结晶。熔点5.5℃,沸点280.5℃(276.4℃),186-187℃(8.8kPa),相对密度1.060(20/4℃),折光率1.602。易溶于乙醇和乙醚,不溶于水。

制备方法:由1-萘酚与乙醇反应而得。将1-萘酚、无水乙醇和浓硫酸混合,加热回流10h以上。然后回收乙醇,将反应物用水洗、碱洗、分出油层。水层用乙醚提取,将提取液与油层合并,用无水氯化钙干燥,回收乙醚后减压蒸馏而得成品。

用途:用于香料制备。

说明:补充资料仅用于学习参考,请勿用于其它任何用途。
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