1) silica gel column
硅胶柱
1.
Effect of reference gas environment in silica gel column on quantitative analysis of CO_2;
硅胶柱上标准气环境对CO_2定量分析的影响
2.
The products of Pulsatilla Saponin produced in enzyme reaction was separated and purified by silica gel column gradient elution.
白头翁皂苷酶解产物经硅胶柱梯度洗脱分离纯化,通过白头翁皂苷酶解产物的第28碳糖基水解反应、TLC和HPLC实验确定:酶解产物Ⅰ为白头翁皂苷Ⅳ,即3 O α L 阿拉伯糖 3β,23 二烃基 Δ20(29) 羽扇豆烯 28 酸,其得率为4。
3.
The purity of isoquercitrin was isolated with a silica gel column.
酶反应产物用硅胶柱层析法提取,可以得到高纯度的异槲皮甙。
2) silica gel column chromatography
硅胶柱层析
1.
Separation and purification of manno-oligosaccharides by silica gel column chromatography;
硅胶柱层析法分离纯化甘露低聚糖
2.
The process of tocopherols purification by silica gel column chromatography;
硅胶柱层析法纯化天然维生素E
3.
Separation of soybean isoflavone aglycones by silica gel column chromatography
硅胶柱层析法分离大豆异黄酮苷元的研究
3) Monolithic silica column
硅胶整体柱
1.
Preparation and Evaluation of Monolithic Silica Columns for Pressurized Capillary Electrochromatography;
加压毛细管电色谱硅胶整体柱的制备及性能评价
2.
Monolithic silica column was prepared by an improved sol-gel technology with tetramethoxysiane and polyethylene glycol as the matrix materials and the influence of modifiers on monolithic silica column was investigated.
研究了改性剂对硅胶整体柱结构性能的影响。
3.
A approach of preparation of monolithic silica column was reported, in which tetramethoxysilane and poly ethylene glycol were used as the material.
研究了硅胶整体柱的制备工艺及温度、pH值对凝胶化过程的影响 ,探讨了凝胶形成的机理 。
4) silica gel chromatography
硅胶柱层析
1.
It was refined by the macroporous adsorption resins and isolated by the silica gel chromatography.
以药用正品北柴胡为原料,经过大孔吸附树脂精制和硅胶柱层析分离纯化,得到纯度大于95%的柴胡皂苷单体。
5) silica gel column chromatography
硅胶柱色谱
1.
Preliminary study on purification of natural tocopherols by silica gel column chromatography;
硅胶柱色谱法提纯天然生育酚的初步研究
6) silica column
硅胶色谱柱
1.
A novel method for the determination of epirubicin by hydrophilic interaction chromatography (HILIC) using high purity silica column with highly polar organic-aqueous buffer as mobile phase has been developed.
采用硅胶色谱柱及高极性有机溶剂水相缓冲溶液流动相。
补充资料:硅胶柱层析
分子式:
CAS号:
性质:以硅胶为固定相的柱色谱法。在经典色谱法中,色谱管为内径均匀、下端缩口的硬质玻璃管,下端用棉花或玻璃纤维塞住,柱管内装入硅胶吸附剂。硅胶的颗粒应尽可能保持均匀,通常直径为:0.07~0.15mm。装柱时将硅胶与流动相相混合,搅拌除去气泡,徐徐倾入色谱柱中。在经典柱色谱中,亦可采用干法装柱。在HPLC中一般采用粒度为5~10fzm的球形或无定形硅胶,柱管长为15~25cm,内径多用0.46cm,采用匀浆法装柱。当采用3恤硅胶时,柱效大于80 000片/m;当采用10μm硅胶时,柱效可大于25 000片/m。它可以进行吸附色谱法的分离,当硅胶含水大于17%时则进行分配色谱法的分离。
CAS号:
性质:以硅胶为固定相的柱色谱法。在经典色谱法中,色谱管为内径均匀、下端缩口的硬质玻璃管,下端用棉花或玻璃纤维塞住,柱管内装入硅胶吸附剂。硅胶的颗粒应尽可能保持均匀,通常直径为:0.07~0.15mm。装柱时将硅胶与流动相相混合,搅拌除去气泡,徐徐倾入色谱柱中。在经典柱色谱中,亦可采用干法装柱。在HPLC中一般采用粒度为5~10fzm的球形或无定形硅胶,柱管长为15~25cm,内径多用0.46cm,采用匀浆法装柱。当采用3恤硅胶时,柱效大于80 000片/m;当采用10μm硅胶时,柱效可大于25 000片/m。它可以进行吸附色谱法的分离,当硅胶含水大于17%时则进行分配色谱法的分离。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。
参考词条