1) crystal aluminum chloride
结晶三氯化铝
1.
Through the experiments and result analysis,this paper discusses the factors influencing the catalytic synthesis of isoamyl acetate with the crystal aluminum chloride as the catalyst.
通过实验及结果分析,讨论了影响结晶三氯化铝催化合成乙酸异戊酯反应的因素。
2) crystalline aluminum chloride
结晶氯化铝
1.
Experimental study was conducted on the preparation of crystalline aluminum chloride from industrial diluted hydrochloric acid and calcium aluminates under atmospheric pressure condition.
通过对常压下采用工业稀盐酸和铝酸钙制备结晶氯化铝净水剂的试验研究,考察了铝酸钙低浓度盐酸浸取时原料配比、浸出时间、浸出温度对三氧化二铝溶出率的影响,并对三氯化铝结晶阶段的机理进行了探讨,实验结果表明低浓度工业废酸可以用于制备结晶氯化铝。
3) hydrate ferric chloride
结晶三氯化铁
4) aluminum chloride
三氯化铝
1.
Chloroxylenol was prepared from 3,5-xylenol and chlorine by using aluminum chloride as catalyst.
以间二甲酚和氯气为原料,在三氯化铝的催化下合成了对氯间二甲酚,最佳工艺条件为:四氯化碳70 mL,60℃下通氯反应90 m in,收率可以达61。
2.
Benzoylacrylic acid was obtained by reacting maleic anhydride with benzene via Friedel-Crafts reaction, in the presence of anhydrous aluminum chloride.
顺丁烯二酸酐与苯在三氯化铝的存在下,经傅-克反应生成苯甲酰丙烯酸,在强酸性水介质中,若温度高于35℃,则部分发生与水的加成反应生成苯甲酰乳酸。
3.
A new method of synthesis of N,N-dimethoxyloneethyl aniline was reported by using anhydrous aluminum chloride, aniline, and methacrylate at lower temperature, the conversion,the yield,and the purity was over 95,91,96 respectively.
报道了用无水三氯化铝作催化剂在低温下将苯胺和丙烯酸甲酯转化为N ,N -二甲氧基羰基乙基苯胺的新方法 ,其反应转化率达 95 %以上 ,产品收率高于 91% ,纯度高于96 % 。
5) aluminium chloride
三氯化铝
1.
The optimum technological factors were studied on the synthesis of 1, 2 - diphenylethane with the reaction of benzene with 1, 2 - dichloroethane catalyzed by anhydrous aluminium chloride.
研究了三氯化铝催化下,1,2-二氯乙烷和苯反应合成1,2-二苯乙烷的最佳工艺条件,结果表明,当苯:二氯乙烷:三氯化铝=10:1:0。
6) aluminium trichloride
三氯化铝
1.
A new process has been developed to synthesize 2 chloro 2′,4′ difluorophenethyl keton from benzene m difluoride and chloro acetic chloride by catalysis of aluminium trichloride, the optimum reaction conditions have been found by orthogonal experimental design, the production rate was over 90%.
以无水三氯化铝作催化剂 ,间二氟苯与氯乙酰氯反应合成 2 -氯 - 2′,4′-二氟苯乙酮。
2.
Solid acid alchlor catalyst was prepared from anhydrous aluminium trichloride through liquid solid solvent method,with pretreated bentonite as support.
以无水三氯化铝为原料 ,并以处理过的膨润土为载体 ,采用液固溶剂法制备固体酸催化剂。
3.
Then the prepared ester is used to synthesize 1,1-cyclopropanedimethanol through reduction with potassium borohydride and aluminium trichloride.
以丙二酸二乙酯为原料,经C-烃化、还原2步得到1,1-环丙二甲醇,其中在C-烃化反应中,用聚乙二醇(PEG)400作为相转移催化剂催化,碳酸钾作用下,与1,2-二氯乙烷反应得到1,1-环丙烷二甲酸二乙酯;在还原反应中,用硼氢化钾还原,在三氯化铝催化下将1,1-环丙烷二甲酸二乙酯还原得到1,1-环丙二甲醇,2步反应总收率50%~55%。
补充资料:结晶氯化铝
分子式: AlCl3·6H2O
CAS号:
性质:无色斜方晶系结晶。工业品为淡黄色或深黄色结晶。密度2.398g/cm3。加热到100℃分解释放出氯化氢。溶于水、无水乙醇、乙醚,微溶于盐酸,其水溶液呈酸性。易潮解,在湿空气中水解生成氯化氢白色烟雾。由煤,碱石粉经沸腾焙烧,再经粉碎后与盐酸反应,经澄清后,把清液浓缩,析出结晶,固液分离制得。主要用于精密铸造模壳的硬化剂,木材防腐剂,造纸施胶沉淀剂,石油工业加氢裂化催化剂单体的原料。也用于羊毛的精制、染色。以及饮用水、含高氟水、工业水的处理,含油污水净化。
CAS号:
性质:无色斜方晶系结晶。工业品为淡黄色或深黄色结晶。密度2.398g/cm3。加热到100℃分解释放出氯化氢。溶于水、无水乙醇、乙醚,微溶于盐酸,其水溶液呈酸性。易潮解,在湿空气中水解生成氯化氢白色烟雾。由煤,碱石粉经沸腾焙烧,再经粉碎后与盐酸反应,经澄清后,把清液浓缩,析出结晶,固液分离制得。主要用于精密铸造模壳的硬化剂,木材防腐剂,造纸施胶沉淀剂,石油工业加氢裂化催化剂单体的原料。也用于羊毛的精制、染色。以及饮用水、含高氟水、工业水的处理,含油污水净化。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。
参考词条