1) benzoyl nitrile
苯甲酰腈
1.
Phenylglyoxylic acid ethyl ester was got via hydrolysis and esterification from benzoyl nitrile in existence of anhydride.
苯甲酰腈在酸酐类催化剂作用下,经水解、酯化得到苯甲酰甲酸乙酯,然后在对甲苯磺酸催化作用下,与乙酰肼反应得到2-乙酰肼基苯甲酰甲酸乙酯,反应总收率为76。
2) benzoyl acetonitrile
苯甲酰乙腈
3) 2-methyl-α-oxobenzoyl cyanide
2-甲基苯甲酰腈
1.
Methyl 2-methyl-(-oxophenylacetate was synthesized by the hydrolysis of 2-methyl-α-oxobenzoyl cyanidewith concentrated sulfuric acid.
2-甲基苯甲酰腈水解制2-甲基-α-氧基苯乙酸甲酯中,物质量比n(2-甲基苯甲酰腈):n(NaCl):n(浓H_2SO_4):n(H_2O)=10∶1∶10∶10,反应温度维持在45℃,反应1。
4) tolyl cyanide
对甲苯磺酰腈
5) 3-benzoylbenzeacetonitrile
3-苯甲酰基苯乙腈
1.
2-(3-Benzoylphenyl)propionitrile which was an important intermediate of ketoprofen was synthesized from 3-benzoylbenzeacetonitrile via monomethylation in the presence of dimethyl carbonate,Pure compound was obtained and the content of crystal was about 99.
以3-苯甲酰基苯乙腈为原料,采用碳酸二甲酯进行α-甲基化反应制备2-(3苯甲酰基苯基)丙腈,使反应控制在单甲基化阶段,HPLC测定产物含量99。
6) 2-(3-benzoylphenyl)propionitrile
2-(3-苯甲酰基苯基)丙腈
补充资料：苯甲酰腈
分子式：C8H5NO
分子量：131.13
CAS号：613-90-1
性质：熔点29-32°C。沸点206°C。闪点84°C。水溶性slihtly soluble, decomposes。
分子量：131.13
CAS号：613-90-1
性质：熔点29-32°C。沸点206°C。闪点84°C。水溶性slihtly soluble, decomposes。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条