1) α-alkylidene cycloketones
N杂α-(芳)亚烷基-环酮
2) N-aryloxazolidones
N-芳基噁唑烷酮
3) N-(α-alkoxyl-alkyl) aromatic amine
N-(α-烷氧基烷基)芳胺
4) 2,3-biarylimino-1,4-dithiacyclohexane
2,3-双芳基亚氨基-1,4-二硫杂环己烷
1.
Five compounds of 2,3-biarylimino-1,4-dithiacyclohexane were prepared by S-alkylation,the structure of them were analyzed by elemental analysis,IR(infrared),1H NMR(nuclear magnetic resonance) and MS(mass spectrometry) preliminarily,and further confirmed by X-ray diffraction.
利用硫原子上的烷基化反应,合成出5个2,3-双芳基亚氨基-1,4-二硫杂环己烷类化合物,由元素分析、红外光谱分析(IR)1、H核磁共振谱分析(1H NMR)、质谱分析(MS)初步确定化合物的结构,并以单晶X射线衍射分析对其结构进一步确证。
2.
Five 2,3-biarylimino-1,4-dithiacyclohexanes were prepared by S-alkylation,the structures of them were analyzed by elemental analysis,IR,~1H NMR and MS preliminarily,and further confirmed by X-ray diffraction.
利用硫原子上的烷基化反应,合成出五个2,3-双芳基亚氨基-1,4-二硫杂环己烷类化合物,由元素分析、红外光谱分析(IR)1、H核磁共振谱分析(1H NMR)、质谱分析(MS)初步确定了化合物的结构,并以单晶X射线衍射分析对其结构进一步确证。
3.
A series of 2,3-biarylimino-1,4-dithiacyclohexane compounds were synthesized by the sufur- alkylation of N,N'-diaryldithiooxamide with 1,2-dibromoethane in the presence of bases.
以N,N'-二芳基二硫代草酰胺与1,2-二溴乙烷进行S烷基化反应,合成了一系列2,3-双芳基亚氨基-1,4-二硫杂环己烷,反应在4h内完成,产率52%～62%。
5) α,α'-bis(arylmethylidene)cycloalkanone
α,α'-双亚苄环烷酮
6) α-nitrocycloalkanone
α-硝基环烷酮
1.
The preparation and application of α-nitrocycloalkanones in organic synthesis are reviewed with reference more than 40.
介绍了α-硝基环烷酮的制备方法,以及它们的特殊反应性和合成应用,参考文献40多篇。
补充资料：[3-(aminosulfonyl)-4-chloro-N-(2.3-dihydro-2-methyl-1H-indol-1-yl)benzamide]
分子式：C16H16ClN3O3S
分子量：365.5
CAS号：26807-65-8
性质：暂无
制备方法：暂无
用途：用于轻、中度原发性高血压。
分子量：365.5
CAS号：26807-65-8
性质：暂无
制备方法：暂无
用途：用于轻、中度原发性高血压。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条