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1)  nicothiazone
尼可硫腙
2)  Nihydrazone
尼海屈腙
3)  Nidroxyzone
尼屈昔腙
4)  Dithizone [dai'θaizəun]
双硫腙
1.
Study on the Adsorption Capability of Barium-Strontium Titanate Powder Coated with Dithizone for Cadmium Ion in Water;
双硫腙包覆钛酸锶钡粉体对水中镉的吸附性能
2.
Determination of Trace Lead Using Solid Silver-Amalgam Electrode Modified with Dithizone by Adsorptive Voltammetry;
双硫腙修饰固体银汞合金电极吸附伏安法测定痕量铅
3.
Determination of Lead in Water Samples by Graphite Furnace Atomic Absorption Spectrometry after Cloud Point Extraction with Dithizone;
双硫腙浊点萃取-石墨炉原子吸收光谱法测定环境水样中痕量铅的研究
5)  diphenylthiocarbazone [,dai,fenil,θaiəu'kɑ:bəzəun]
双硫腙
1.
Simultaneous Determination of Lead and Zinc in Natural Water by Flame Atomic Absorption Spectrometry with Microemulsion Sampling and Diphenylthiocarbazone Liquid-Liquid Extraction;
双硫腙四氯化碳萃取微乳液进样火焰原子吸收光谱法同时测定天然水中的铅和锌
2.
Colorimetry to determinate the micro lead in the bee glue with diphenylthiocarbazone has no potassium cyanide;
无氰化钾双硫腙比色法测定蜂胶中微量铅
3.
The method of using diphenylthiocarbazone-chloroform-benzene mixed solvent to determine the content of silver in the ore by extraction colorimetric is introduced in this paper.
双硫腙-氯仿-苯混合溶剂萃取比色测定矿石中的银。
6)  dithizone [dai'θaizəun]
二苯硫腙
1.
7, EDTA as a masking agent, silver was indirectly determined by extraction spectrophotometry with dithizone CCl 4.
稀硝酸溶样后用 0 1mol/L硝酸定量稀释到一定浓度 ,以EDTA作掩蔽剂 ,控制溶液 pH4 7,以二苯硫腙的四氯化碳溶液萃取分光光度法间接测定粗铅中银的含量 ,可测定约 0 3 %含银量 ,操作快速 ,便于推
2.
In this paper an extraction catalytic kinetic spec-trometric method for the determination of trace palla-dium(Ⅱ)has been described, based on the fact thatpalladium(Ⅱ)can catalyse the oxidation of dithizone by oxygen in the presence of 1,10-phenanthroline asan activator.
O的缓冲溶液中,利用邻菲罗嘛活化Pd(Ⅱ)催化水中溶解氧氧化二苯硫腙褪色的指示反应,建立了测定痕量钯的萃取催化动力学分析方法。
补充资料:双硫腙
分子式:C13H12N4S
分子量:256.33
CAS号:60-10-6

性质:蓝黑色结晶性粉末。熔点165-169℃(分解)。易溶于氯仿、四氯化碳,稍溶于醇,不溶于水。

制备方法:按下述步骤制备。1.苯肼二硫代甲酸苯肼盐的制备。将13g苯肼溶于60ml乙醚中,滴加5.2ml二硫化碳。将生成的白色沉淀滤出,用乙醚洗涤,得约15g。2.二苯二氨基硫脲的制备。将上述生成物置于烧杯中,在96-98℃的水浴上加热,物料熔融后放出硫化氢而转为淡黄以的胶状物。若有氨气放出,则移出热浴,用水冷却。再用冰冷却。再用冰冷却,加入15ml水无水乙醇,自冰浴中取出,搅拌下稍热,这时胶状物变成结晶状产物,抽滤,用乙醇洗涤,得约7.5g。3.双硫腙的制备。将上述所得二苯二氨基硫脲加到苛性钾溶液(6g氢氧化钾溶于60ml无水甲醇)中,在沸水浴上回流5min,取出在冰浴中冷却。过滤,滤液用硫酸酸化至刚果红试纸变色,析出深蓝色沉淀。抽滤,将沉淀物再用苛性钾溶液、硫酸处理一遍,抽滤后用水洗至无硫酸根存在。在40℃烘干,得双硫腙约3g。

用途:该品是测定微量沿的络合指示剂,并用于测定钴、铜、汞、锌和银等。

说明:补充资料仅用于学习参考,请勿用于其它任何用途。
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