1) 4-Bromo-3-nitroanisole
4-溴-3-硝基苯甲醚
2) 3-Nitro-4-bromoanisloe
3-硝基-4-溴苯甲醚
3) 5-Methoxy-2-nitrotoluene
3-甲基-4-硝基苯甲醚
4) 4-methyl-3-nitroanisole
4-甲基-3-硝基苯甲醚
5) 4-Bromomethyl-3-nitrobenzoic acid
4-溴甲基-3-硝基苯甲酸
6) 2-bromo-4-nitroanisole
2-溴-4-硝基苯甲醚
1.
2-Bromo-4-nitrophenol was synthesized by using 2-methoxy-5-nitroaniline as the starting material via diazotization reaction and the Sandmeyer reaction to yield 2-bromo-4-nitroanisole,which was further treated with sodium hydroxide to realize a nucleophilic substitution reaction,with the product acidified by hydrochloric acid to obtain the desired product 2-bromo-4-nitrophenol.
以2-甲氧基-5-硝基苯胺为原料经重氮化、Sandmeyer反应得到2-溴-4-硝基苯甲醚,再与氢氧化钠发生亲核取代反应,经盐酸水解得到标题化合物,总收率达55。
补充资料：4-溴-3-硝基苯甲醚
CAS: 5344-78-5
沸点: 153℃
熔点: 32-34℃
中文名称: 4-溴-3-硝基苯甲醚
英文名称: 4-Bromo-3-nitroanisole
沸点: 153℃
熔点: 32-34℃
中文名称: 4-溴-3-硝基苯甲醚
英文名称: 4-Bromo-3-nitroanisole
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条