1) dioxane-2,3-dlol
2,3-二羟基-1,4-二氧杂环己烷
2) p-dioxane
1,4-二氧杂环己烷
3) 2,3-biarylimino-1,4-dithiacyclohexane
2,3-双芳基亚氨基-1,4-二硫杂环己烷
1.
Five compounds of 2,3-biarylimino-1,4-dithiacyclohexane were prepared by S-alkylation,the structure of them were analyzed by elemental analysis,IR(infrared),1H NMR(nuclear magnetic resonance) and MS(mass spectrometry) preliminarily,and further confirmed by X-ray diffraction.
利用硫原子上的烷基化反应,合成出5个2,3-双芳基亚氨基-1,4-二硫杂环己烷类化合物,由元素分析、红外光谱分析(IR)1、H核磁共振谱分析(1H NMR)、质谱分析(MS)初步确定化合物的结构,并以单晶X射线衍射分析对其结构进一步确证。
2.
Five 2,3-biarylimino-1,4-dithiacyclohexanes were prepared by S-alkylation,the structures of them were analyzed by elemental analysis,IR,~1H NMR and MS preliminarily,and further confirmed by X-ray diffraction.
利用硫原子上的烷基化反应,合成出五个2,3-双芳基亚氨基-1,4-二硫杂环己烷类化合物,由元素分析、红外光谱分析(IR)1、H核磁共振谱分析(1H NMR)、质谱分析(MS)初步确定了化合物的结构,并以单晶X射线衍射分析对其结构进一步确证。
3.
A series of 2,3-biarylimino-1,4-dithiacyclohexane compounds were synthesized by the sufur- alkylation of N,N'-diaryldithiooxamide with 1,2-dibromoethane in the presence of bases.
以N,N'-二芳基二硫代草酰胺与1,2-二溴乙烷进行S烷基化反应,合成了一系列2,3-双芳基亚氨基-1,4-二硫杂环己烷,反应在4h内完成,产率52%～62%。
4) 8-(4-oxocyclohexyl)-1,4-dioxaspiro[4.5]decane
8-(4-氧代环己烷基)-1,4-二氧杂螺[4.5]癸烷
5) 1,4-Bis(hydroxymethyl)-cyclohexane
1,4-二(羟甲基)环己烷
6) (generic)phosphoramide
1,6-二(2,3-环氧丙基)己烷
补充资料：2,3-二羟基-1,4-二氧杂环己烷
CAS: 4845-50-5
分子式: C4H8O4
熔点: 91-95℃
中文名称: 2,3-二羟基-1,4-二氧杂环己烷
英文名称: 1,4-Dioxane-2,3-diol；trans-2,3-dihydroxy-1,4-dioxane；dioxane-2,3-dlol
分子式: C4H8O4
熔点: 91-95℃
中文名称: 2,3-二羟基-1,4-二氧杂环己烷
英文名称: 1,4-Dioxane-2,3-diol；trans-2,3-dihydroxy-1,4-dioxane；dioxane-2,3-dlol
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
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