1) 2-acetyl-1,4,5,6-tetratydropyridine
2-乙酰基-1,4,5,6-四氢吡啶
2) 1,4,5,6-Tetrahydro-1,2-dimethylpyrimidine
1,4,5,6-四氢-1,2-二甲基嘧啶
3) Methyl 2-pyridyl ketone
2-乙酰基吡啶
4) 3-(2-Chloroethyl)-6,7,8,9-tetrahydro-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one
3-(2-氯乙基)-6,7,8,9-四氢-2-甲基-4H-吡啶并[1,2-a]嘧啶-4-酮
5) 2-carbethoxy-6-acetylpyridine
2-乙酯基-6-乙酰基吡啶
1.
A new unsymmetric compound 2-carbethoxy-6-acetylpyridine (4) was synthesized from the starting material 2,6-dimethylpyridine through four reaction steps, and then a series of 6-acetylpyridine-2-carboxamides 5～7 were prepared by the microwave irradiation from the precursor 4.
2,6-二甲基吡啶经氧化、酯化、Claisen酯缩合后制得新型化合物2-乙酯基-6-乙酰基吡啶(4),用其作为前驱体,与一系列小分子脂肪胺:甲胺、乙胺、乙二胺在微波条件下生成3个吡啶酰胺化合物5,6,7。
6) 2-acetylpyridine
2-乙酰吡啶
1.
Synthesis and crystallographic structural studies on two mononuclear complexes of Co(Ⅱ),Ni(Ⅱ) from 2-acetylpyridine and ethanolamine;
Co(II)和Ni(II)2-乙酰吡啶乙醇胺配合物合成与结构
2.
3-(4-Methylphenyl)-1,5-di(2-pyridyl)-1,5-pentadione was prepared by reaction of 2-acetylpyridine with 4-methylbenzaldehyde at room temperature using ethanol as the solvent,followed by reacting with concentrated ammonia for 1 h in the presence of sodium hydroxide and the final product 4-tolyl-2,2′:6′,2″-terpyridine was obtained with a total yield of 31.
以2-乙酰吡啶和对甲基苯甲醛为原料,在室温下的乙醇溶液中制得3-(4-甲基苯)-1,5-二(2-吡啶基)-1,5-戊二酮,后者在氢氧化钠存在下与浓氨水反应1 h得到标题化合物,总产率31。
3.
A novel binuclear nickel(Ⅱ) complex C17H20N4Ni(H2O)Cl2Cl2·(CH3OH) with organic ligands of 2-acetylpyridine and 1,2-propylenediamine has been one-pot synthesized and characterized by means of elemental analysis,IR and single crystal X-ray diffraction.
采用"一锅煮"方法,在金属Ni(Ⅱ)离子作用下,以2-乙酰吡啶和1,2-丙二胺物质的量比为2∶1进行反应,得到了一种新的闭环单Schiff碱N4四齿配体的配合物[C17H20N4Ni(H2O)Cl]2Cl2·(CH3OH)。
补充资料：2-乙酰基吡啶
分子式：C7H7NO
分子量：121.13
CAS号：1122-62-9
性质：密度1.08。熔点8-10°C。沸点188-189°C。折射率1.52-1.522。闪点76°C。
分子量：121.13
CAS号：1122-62-9
性质：密度1.08。熔点8-10°C。沸点188-189°C。折射率1.52-1.522。闪点76°C。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
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