In recent years the development of hardware template method can use pre-forming mesoporous solid and orderly channel structure,soaking the foot of inorganic salt precursor through two or more times to obtain a new mesoporous material,which is a mesoporous oxide material.

In this paper,the synthetic methods of mesoporous metal oxides /composites are reviewed,which can be divided into three kinds of methods: soft template route,hard template route and nanocrystal assembly route.

The recent progress in studies of non-siliceous mesoporous materials including mesoporous aluminophosphates (AlPOs), mesoporous carbon and mesoporous metal oxides are reviewed.

In this paper,the synthesis and investigation of several types of non silica mesoporous materials,including mesoporous carbon,mesoporous metal oxides,and mesoporous metals,are introduced,their characterization and application are also reviewed.

In this thesis, we chose several mesoporous solids as hard template for preparing some mesoporous metal oxides such as indium oxides, tin oxides, indium and tin oxide composite and copper oxide.

The results of electrochemical tests show that the mesoporous metal oxides have fine supercapacitive behaviors and their specific capacitance values at the discharging current of 5 mA are 176 and 298 F·g-1, respectively.