1) Clozapine
氯氯平
2) o-chlorobenzyl chloride
邻氯氯苄
1.
The preparation of o-chlorobenzaldehyde from the residual liquid generated in the production of o-chlorobenzyl chloride;
由生产邻氯氯苄的残液制备邻氯苯甲醛
2.
According to the main problem of current synthesis of o-chlorobenzyl chloride in our country,effective improvement was studied to increase the reaction conversion to 60% by use of a new catalyst CHJ-3.
针对目前国内邻氯氯苄生产工艺存在的主要问题,通过选用新型催化剂CHJ-3,改进催化氯化工艺,使氯化反应邻氯甲苯转化率达到60%。
3.
Taking o-cholorotoluene as raw material,the factors influencing the photochlorination synthesis of the o-chlorobenzyl chloride were investigated.
研究了邻氯甲苯光氯化生成邻氯氯苄的各项影响因素,在适宜条件下,邻氯甲苯的转化率可达75%以上,反应过程邻氯氯苄的收率可达90%。
3) 2-chlorobenzyl chloride
邻氯氯苄
1.
A gas chromatography with n-tridencame as the internal strandard was used for determing the content of industrial 2-chlorobenzyl chloride.
采用气相色谱内标法,以正十三烷作内标物,测定工业邻氯氯苄的含量。
2.
According to the key problems of current domestic synthesis process of 2-Chlorobenzyl Chloride, effective improvement had been studied by applying advanced reaction rectification technology to increase the reaction conversion to 78%; Therefore, the production cost was reduced.
针对目前国内邻氯氯苄生产工艺存在的主要问题,通过采用先进的反应精馏技术,改进氯化合成工艺,将反应转化率提高到78%,从而有效地降低了生产成本,经济效益和社会效益显著,具有很好推广应用前景。
4) 4-chlorobenzyl chloride
对氯氯苄
1.
The influence of reaction temperature,the molar ratio of trimethyl phosphite to 4-chlorobenzyl chloride,reaction time and feeding mode on the yield of p-chlorobenzyl phosphate was investigated.
以亚磷酸三甲酯和对氯氯苄为原料,通过Arbuzov重排反应制得了对氯苄基磷酸酯。
2.
p-chlorobenzyl) pyridine is prepared from 4-chlorobenzyl chloride and pyridine hydrochloride via condensation.
以对氯氯苄与盐酸吡啶缩合法制备 2 -对氯苄基吡啶 。
5) dichlorobenzyl chloride
二氯氯苄
6) p-chlorobenzyl chloride
对氯氯苯
参考词条
补充资料:氯氧平
分子式:C17H16ClN3O
分子量:313.79
CAS号:14028-44-5
性质:熔点313.5℃。
制备方法:氯甲酸乙酯和邻-(对氯苯氧基)苯胺盐酸盐反应制取邻-(对氯苯氧基)苯氨基甲酸乙酯,再使其与N-乙酯基哌嗪反应,生成4-[[邻-(对氯苯氧基)苯基]氨基甲酰]-1-哌嗪羧酸乙酯,将此哌嗪羧酸酯和五氧化二磷、三氯氧磷一起加热回流,环合得到氯氧平。
用途:抗忧郁药。
分子量:313.79
CAS号:14028-44-5
性质:熔点313.5℃。
制备方法:氯甲酸乙酯和邻-(对氯苯氧基)苯胺盐酸盐反应制取邻-(对氯苯氧基)苯氨基甲酸乙酯,再使其与N-乙酯基哌嗪反应,生成4-[[邻-(对氯苯氧基)苯基]氨基甲酰]-1-哌嗪羧酸乙酯,将此哌嗪羧酸酯和五氧化二磷、三氯氧磷一起加热回流,环合得到氯氧平。
用途:抗忧郁药。
说明:补充资料仅用于学习参考,请勿用于其它任何用途。