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1)  solid-phase reactor
固相反应器
1.
Determination of content and dissolution of estazolam tablets by flow injection spectrofluorometry with solid-phase reactor;
固相反应器流动注射在线氧化荧光法测定艾司唑仑片剂含量及溶出度
2.
In this paper, NaBiO_3 with strong oxidation property was immobilized on the silica gels and applied in flow system flow injection system and sequential injection system as solid-phase reactor.
固相反应器基于其节省试剂、实验装置简化、操作简单和提高分析体系灵敏度等特点,目前已经越来越多地与流动体系相结合并被用于药物分析、环境分析和生物分子的测定中。
3.
Methods:Estazolam was oxidized on-line into a strongly fluorescent compound with a lead dioxide solid-phase reactor,then the content of estazolam was determined with a fluorimetric detector in flow injection system.
方法:利用二氧化铅固相反应器在线氧化艾司唑仑为强荧光化合物,流动注射荧光法测定艾司唑仑含量;以中国药典溶出度测定的溶出条件,建立自动采样、测定的溶出度测定方法。
2)  solid state reaction
固相反应
1.
Study on synthesis and crystallization degree of Cu~(2+)-doped lithium zinc phosphate by solid state reaction;
固相反应合成掺铜磷酸锌锂及其结晶度的研究
2.
Synthesis and characterization of SnO_2 nanorods prepared by solid state reaction;
SnO_2纳米棒的固相反应制备与表征
3.
The preparation of nano-complosite oxide solid solution of cerium and zirconium by solid state reaction;
固相反应法制备纳米铈锆复合氧化物
3)  solid reaction
固相反应
1.
Study on the Solid Reaction between CuSO 4·5H 2O and KBr in KBr Pellets;
CuSO_4·5H_2O在用KBr压片法制样时所发生的固相反应的研究
2.
C4A3S is formed mainly by solid reaction of CaO, Al2O3 and CaSO4 below 1 100 ℃.
研究表明:C4A3S矿物分别是通过3种不同途径形成的;在煅烧温度低于1100℃时,C4A3S矿物主要是由CaO,Al2O3,CaSO4直接通过固相反应形成;在煅烧温度高于1100℃时,C4A3S矿物是通过中间矿相七铝酸十二钙(C12A7)或铝酸一钙(CA)的形成而形成的。
3.
ZnS:Mn phosphor particles were prepared by solid reaction with ZnS and MnCl_2·4H_2O.
以ZnS(荧光纯)与MnCl2(分析纯)为原料通过固相反应法,高温烧结制成ZnS:Mn荧光粉。
4)  Solid-phase reaction
固相反应
1.
Solid-phase reaction between high purity magnesia and chrome ore from Tibet;
高纯镁砂与西藏铬矿间固相反应的研究
2.
The results showed that the thermodynamic conditions are available to the solid-phase reaction of NiO with Fe_2O_3, and the solid-phase reaction goes on with the densification process though the f.
研究以NiO和Fe2O3为主要原料合成镍铁尖晶石反应烧结过程中的热力学条件·同时对在不同烧结条件下合成的尖晶石二次烧结制备的阳极试样的抗弯强度及高温电导率进行了测量·结果表明:NiO和Fe2O3固相反应的热力学条件具备,反应先于致密化过程结束·当未经压制成型的粉料直接在合成温度为900℃下合成6h,经破碎工艺及二次烧结后,所制得的惰性阳极试样强度及电导率最大,烧结性能最好·而破碎工艺对增加粉末活性,提高试样电导率及力学性能也十分重要
3.
The result revealed that an intensive solid-phase reaction occurs on the composite\'s interface between SiC and 20Cr steel,then SiC decomposed into Si that forms Fe-Si compound with Fe and C that precipitated in graphite form.
结果表明:SiC和20Cr在复合材料的界面产生较强固相反应,SiC分解出的Si与Fe结合生成Fe-Si化合物,SiC分解出的C以石墨态沉积下来。
5)  solid-state reaction
固相反应
1.
Preparation of nanometer NiO by solid-state reaction at low temperature;
低热固相反应合成纳米氧化镍
2.
Preparation of nanometric Co_3O_4 by solid-state reaction and sublimating NH_4Cl;
固相反应共生-升华氯化铵法制备纳米四氧化三钴
3.
Influence of fabrication conditions on transparency of YAG polycrystalline by solid-state reaction method;
制备条件对固相反应法制取YAG多晶体透光性的影响
6)  solid phase reaction
固相反应
1.
Study on reducing silver through solid phase reaction;
固相反应还原银的研究(Ⅰ)
2.
Study on reducing silver through solid phase reaction();
固相反应还原银的研究(Ⅱ)
3.
Investigation of Co/Si/Ti/Si and Co/Si…/Ti/Si Multilayer Solid Phase Reaction Applied in Self\|Aligned Elevated Silicide Structure;
用于自对准提升硅化物结构的Co/Si/Ti/Si及Co/Si/…Ti/Si多层薄膜固相反应研究
补充资料:固固相反应过程
      两种固相反应物之间进行的多相反应过程,按反应机理,可分为真固固相反应和假固固相反应。
  
  真固固相反应  两种粉末状固相反应物直接接触进行反应,包括:①固固相化合反应,如四氧化三钴与氧化锌反应生成绿色颜料林曼绿。②固固相交换反应,如氧化钡与碳酸钙反应生成碳酸钡和氧化钙。具有现实工业价值的是一系列在低温下用碳使金属氧化物还原而生成金属或金属碳化物的反应。例如:
  
  
  
   TiO2+3C─→TiC+2CO
  
  固固相反应是通过固相内部原子(包括离子、电子和空穴)的迁移而实现的。固固相反应的速率取决于原子的扩散系数和产物层的化学位梯度。MgO和Fe2O3反应生成铁酸镁的过程(见图)是真固固相反应的实例,物质的迁移是这种反应的一种机理。
  
  假固固相反应  高温下两种固相反应物借助于气相中间物进行的反应。例如用碳使氧化铁还原是通过气相中间物而进行的,其机理为:
  
  
  
  
  FeO+CO─→Fe+CO2
  
  
  
  
  C+CO2─→2CO两个气固相反应构成:
  
  
  
  
  FeO+C─→Fe+CO因此,可利用气固相反应的某些研究成果进行分析。
  

说明:补充资料仅用于学习参考,请勿用于其它任何用途。
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