1) aqueous phase
水溶剂法
1.
The optimum reaction conditions via aqueous phase were investigated,and the yield and purity of chlorpyrifos were over 95% and 97% respectively.
以2,3,5,6-四氯吡啶和液碱为原料,一步制得3,5,6-三氯吡啶醇钠,3,5,6-三氯吡啶醇钠和O,O-二乙基硫代磷酰氯反应得到目标产物,报道了一种用三元复合催化剂催化合成毒死蜱的新方法,探讨了采用水溶剂法合成毒死蜱的适宜的工艺条件,毒死蜱的收率、质量分数分别达到95%和97%以上,并采用IR、1H NMR对该化合物的结构进行了表征。
2.
The optimum reaction conditions via aqueous phase were investigated.
本文研究了水溶剂法合成毒死蜱的工艺。
2) water solvent
水溶剂法
1.
The monostearic sucrose ester was synthesized with water solvent, optimal condition sucrose: fatty acid glyceride = 3∶1(mole Ratio); emulsifying agent 5%, catalyst 5%,water 10% (based on the weight of main reactants); reation time 4 h, temperature 150 ℃, vacuum 0.
采用水溶剂法合成蔗糖单硬脂酸酯适宜的反应条件为 :蔗糖与硬脂酸单甘酯摩尔比为 3∶ 1、乳化剂用量5%、催化剂用量 5%、水用量 10 %、反应温度 150℃、反应时间 4 h、压力 0 。
3) non-aqueous solvent method
非水溶剂法
1.
Copper sulfide nanoparticles and nanorods were synthesized at ambient conditions via a novel non-aqueous solvent method that employed ethanol as solvent and sodium dodecyl benzene sulfonate (SDBS) as surfactant.
以无水乙醇为溶剂,SDBS为表面活性剂,采用一种便利的非水溶剂法,在常温常压下合成了硫化铜纳米球和纳米棒。
4) solvent-assisted hydrothermal method
溶剂助水热法
5) hydrolysis solvothermal method
水解溶剂热法
1.
Nanometer titanias in different crystal structures with high specific surface area have been prepared by the hydrolysis solvothermal method usi.
本文以钛酸丁酯为原料，在酸性条件下，通过醇盐水解溶剂热法可控地合成了具有较高比表面积的金红石型和锐钛矿型混合晶型的纳米TiO_2粉体。
6) hydrothermal-solvothermal method
水热-溶剂热法
1.
In this paper, by using the hydrothermal-solvothermal method, CdS quantum dots with excellent fluorescence property were synthesized.
本文采用水热-溶剂热法制备了荧光性能强的CdS量子点,并讨论了制备条件对CdS量子点晶型、形貌和荧光性能的影响,为开发CdS量子点作为生物标记物提供必要的理论基础。
补充资料：等水溶剂
分子式：
CAS号：
性质：在液固色谱法中，调配一定含水量的、不引起吸附剂活性变化的流动相。
CAS号：
性质：在液固色谱法中，调配一定含水量的、不引起吸附剂活性变化的流动相。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条