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1)  floating catalytic pyrolysis method
浮动催化热分解法
1.
Multi-wall carbon nanotubes(MWNT) were preparaed by floating catalytic pyrolysis method,using liquid paraffin as the carbon source,ferrocene as the precursor of catalyst and dimethyl sulfoxide as the growth accelerant.
以无毒的液体石蜡为碳源、二茂铁为催化剂前驱体、含硫化合物二甲基亚砜为生长促进剂,采用浮动催化热分解法制备多壁碳纳米管,通过TEM、SEM、XRD、Ram an、TG等对产物形貌和结构进行了表征。
2)  floating catalyst method
浮动催化裂解法
1.
Byproducts of floating catalyst method for preparing carbon nanotubes;
浮动催化裂解法制备碳纳米管的副产物
2.
The synthesis of single-walled carbon nanotubes(SWNTs)by floating catalyst method,using phos- phorus as promoter,was investigated.
采用浮动催化裂解法研究了磷作为促进剂对SWNTs制备的影响。
3.
Carbon nanotubes with good quality were prepared continuously in a vertical reactor by floating catalyst method, in which the catalyst precursor was directly carried into the reactor by a gas flow, thus avoiding the tedious step of catalyst preparation.
改进了原有立式浮动催化裂解法制备碳纳米管的装置与工艺,省略了繁琐的催化剂制备工艺,催化剂前驱体在气体带动下直接进入反应器,实现了连续化制备碳纳米管,产量约为4 g/h,纯度达80%。
3)  floating catalyst method
流动催化热分解法
1.
Optimization for preparation of carbon nanotubes by floating catalyst method;
流动催化热分解法制备碳纳米管工艺条件的正交优化
4)  floating catalytic pyrolysis
流动催化热解法
1.
High-quality multiwalled carbon nanotubes prepared by the floating catalytic pyrolysis;
流动催化热解法制备高质量多壁碳纳米管的研究
5)  catalytic decomposition method
催化热分解法
1.
Arc-discharge and catalytic decomposition methods were used to produce carbon nanotubules.
采用直流电弧法和催化热分解法制备出了纳米碳管,并对这两种方法的工艺进行了初步的探讨,获得了工艺流程和工艺参数。
6)  floating catalyst method
浮动催化法
1.
The continuous synthesis was realized by controling parameters using floating catalyst method.
报道了竹节状纳米碳管的连续合成,通过对生长因素的控制可以用浮动催化法连续合成竹节状纳米碳管。
2.
The carbon micro/nano-materials with different morphologies are synthesized in a single horizontal high-temperature resistance furnace by floating catalyst method with a reaction system using ethanol as the carbon source,through varying the experimental factors such as the types of the catalysts,the kinds and flow rates of the reaction gases and additives.
采用浮动催化法,利用卧式单一高温电阻炉,在以无水乙醇为碳源的反应体系中通过改变催化剂、反应气氛及流量、添加剂等实验参数合成了形貌不一的碳微纳米材料;采用SEM和Raman对产物进行了形貌观察和表征;比较了这些实验参数对浮动催化法制备碳纳米管的影响,并对其作用机理进行了简单分析。
补充资料:中压压热釜非催化油脂水解法
分子式:
CAS号:

性质:一种使用很广的油脂水解工艺方法。当油脂与水的反应温度达到225℃,就可以无需催化剂进行水解而达到较高的反应速率,并实现连续化。操作压力要高于反应温度下的饱和压力(不低于3MPa),以保持反应系统处于液相状态。反应过程是逆流的,并分为3段进行。每段都经过静置分层以降低油相中的甘油含量,有利于提高水解率,最终可达到97%。已实现工业化的方法有多种。使用较多的有Gianazza法和Construzioni Meccaniche Bernardini法。

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