1) diglycolic acid
二甘醇酸
1.
A new lanthanide coordination polymer {[Dy2(dga)3(H2O)4]·2H2O}n was prepared by hydrothermal method with DyCl3·6H2O and diglycolic acid(H2dga),and structurally characterized by single-crystal X-ray diffraction technique.
6H2O与二甘醇酸(H2dga)在水热条件下反应得到配位聚合物{[Dy2(dga)3(H2O)4]。
2.
A mixture of diglycolic acid with chiral 2-amino-1-butanol or L-phenylalaninol was dehydrated for 23 h when being refluxed in toluene to form via an one-step reaction(R)-or(S)-1,5-bis[2′-(4′-ethyloxazolinyl)]methyl ether and(S)-1,5bis[2′-(4′-benzyloxazolinyl)] methyl ether with their yields in the range of 91.
二甘醇酸与手性2-氨基-1-丁醇或L-苯丙氨醇在甲苯中回流脱水23 h,一步反应合成了(R)-或(S)-1,5-双-[2-′(4′-乙基噁唑啉)]甲醚和(S)-1,5-双-[2-′(4′-苄基噁唑啉)]甲醚,产率为91。
2) dimethyl diglycolate
二甘醇酸二甲酯
1.
A mixture of 1,2-carbonyl compounds(glyoxal trimer dihydrate,diethyl oxalate or benzil) with dimethyl diglycolate is refluxed via condensation for 6~8h in cyclohexane in the presence of KOH,and give furan-2,5-dicarboxylic acid,3,4-dihydroxyfuran-2,5-dicarboxylic acid and 3,4-diphenylfuran-2,5-dicarboxylic acid in the yields of 73.
在KOH的作用下,1,2-二羰基化合物二水合三聚乙二醛、草酸二乙酯或二苯乙二酮与二甘醇酸二甲酯在环己烷中回流6~8h,缩合成呋喃-2,5-二甲酸、3,4-二羟基呋喃-2,5-二甲酸和3,4-二苯基呋喃-2,5-二甲酸,产率为73。
3) Diglycol diacetate
二甘醇二醋酸酯
1.
Diglycol diacetate had been obtained with sulfuric acid or toluene-p-sulfonic acid as catalyst in lab.
研究了在实验室条件下 ,以硫酸、对甲苯磺酸为催化剂合成二甘醇二醋酸酯的方法。
4) diethylene glycol dipropionate
二甘醇二丙酸酯
5) diethylene glycol dipelargonate
二甘醇二壬酸酯
6) Diethyleneglycol diformate
二甘醇二甲酸酯
补充资料:二甘醇酸
CAS: 110-99-6
分子式:C4H6O5
分子质量:134.08
熔点: 141-145℃
中文名称: 二甘醇酸;一缩二乙二醇酸;一缩二乙醇酸
英文名称: 2,2'-oxybis-Acetic acid;oxydi-acetic aci;2,2'-oxybisacetic acid;2,2'-oxydiacetic acid;3-oxapentanedioic acid;2,2'-oxybis-acetic aci;bis(carboxymethyl)ether;diglycolic acid;oxodiacetic acid
分子式:C4H6O5
分子质量:134.08
熔点: 141-145℃
中文名称: 二甘醇酸;一缩二乙二醇酸;一缩二乙醇酸
英文名称: 2,2'-oxybis-Acetic acid;oxydi-acetic aci;2,2'-oxybisacetic acid;2,2'-oxydiacetic acid;3-oxapentanedioic acid;2,2'-oxybis-acetic aci;bis(carboxymethyl)ether;diglycolic acid;oxodiacetic acid
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