1) headspace sampling-capillary column
顶空进样-毛细管柱
2) headspace capillary gas chromatography
顶空毛细管柱气相色谱法
1.
The method for determining the content of residual solvents ethanol,dichloromethane,ethyl acetate,pyridine in isradipine by headspace capillary gas chromatography was developed with a good linearity.
建立测定伊拉地平中有机溶剂乙醇、二氯甲烷、乙酸乙酯、吡啶残留量的顶空毛细管柱气相色谱法。
3) open hole capillary column
空心毛细管柱
4) headspace injection
顶空进样
1.
A capillary column headspace injection method for the determination of residual methanol, tetrahydrofuran, dichloroethane, pyridine and toluene in reloxifene hydrochloride was established.
采用毛细管柱顶空进样法 ,以二烷为内标 ,同时测量盐酸雷洛昔芬中甲醇、四氢呋喃、二氯乙烷、吡啶及甲苯等 5种溶剂的残留量。
2.
A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.
建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ,N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。
3.
Methods The volatile compounds obtained by steam distillation or direct headspace injection were analyzed by GC-MS.
方法采用传统的水蒸气蒸馏提取挥发油,和顶空进样直接采集挥发性成分2种方法,对吉林细辛中的挥发性成分进行GC-MS分析。
5) Headspace
[英]['hedspeis] [美]['hɛd,spes]
顶空进样
1.
A method for the determination of volatile constituents in adhesive by headspace GC/MS was proposed.
报道利用顶空进样 -GC/MS技术鉴定物质中挥发性成份的方法 ,鉴定出XY挥发性成份。
2.
Determination of residual solvent in medicine by wide-bore capillary Headspace-Gas Chromatography(HS-GC)is a rapid,simple and high-efficient method,it is widely applicated to determinate residual solvent in medicine.
本文通过建立原料药肝素钠、烟酸占替诺、福辛普利钠和盐酸头孢唑兰中残留溶剂分析测定方法,阐述了顶空进样一大口径毛细管气相色谱法检测药物中残留溶剂的应用,通过研究建立方法,探讨了顶空进样大口径毛细管气相色谱法应用开发和实际应用问题。
3.
METHODS The headspace GC system consisted of a capillary column,polymerization or cross linking polyethylene glycol as the solid phase,and FID as the detector.
方法以聚乙二醇为固定相的毛细管色谱柱,氢火焰离子检测器,顶空进样方式,柱温:起始温度为60℃,程序升温起始温度为60℃,保持16 min,以每分钟20℃的升温速率升至200℃,保持2 min。
6) Headspace Sampling
顶空进样
1.
Determination of the residual organic volatile solvents in block cream by gas chromatography with headspace sampling;
气相色谱顶空进样法测定防晒霜中有机溶剂残留量
2.
Determination of three residual organic volatile solvents in cefepime by gas chromatography with headspace sampling;
气相色谱顶空进样法测定头孢吡肟中3种有机物残留量
3.
In concentrated sulfuric acid TFA may change into MTFA with dimethyl sulfate(DMS),so it is possible to obtain the mass concentration of TFA in water samples by determining the mass concentration of MTFA with headspace sampling and GC-MS,using the volatility of MTFA.
笔者建立了测定TFA质量浓度的实验方法:将样品中的三氟乙酸与硫酸二甲酯在浓硫酸介质中衍生为三氟乙酸甲酯(MTFA),利用MTFA的易挥发性,以顶空进样和气相色谱-质谱联用的方法检测样品中MTFA的质量浓度,进而得到环境水样中TFA的质量浓度。
补充资料：微升点样毛细管
分子式：
CAS号：
性质：薄层色谱中的一种定量点样容器，通常规格有0.5、1、2、3、4、5和l0μl等，由顶端开一小孔的橡皮滴头、玻璃管、橡皮塞及可按点样要求更换各种规格的定量玻璃毛细管组成。除玻璃毛细管外，也有铂铱合金制的毛细管，通常规格有100、200nl，一般作为自动点样器的附件。微升毛细血管的优点是使用方便、点样准确度高、价格便宜。
CAS号：
性质：薄层色谱中的一种定量点样容器，通常规格有0.5、1、2、3、4、5和l0μl等，由顶端开一小孔的橡皮滴头、玻璃管、橡皮塞及可按点样要求更换各种规格的定量玻璃毛细管组成。除玻璃毛细管外，也有铂铱合金制的毛细管，通常规格有100、200nl，一般作为自动点样器的附件。微升毛细血管的优点是使用方便、点样准确度高、价格便宜。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条