1) α-naphthalene acyl
萘乙酰基
1.
Eight novel N,N′-naphthalene acyl substituted aromatic acylamino thiocarbamides(Ⅱ1~Ⅱ8) were synthesized from aryl acylhydrazine(Ⅰ) and α-naphthalene acyl isothiocyanate, which was obtained by the reaction of potassium thiocyanate with α-naphthalene acyl chloride obtained from 2-naphthylacetic acid and thionyl chloride in anhydrous benzene.
通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与芳基酰肼进行加成反应,合成8种新型N,N′-萘乙酰基取代芳乙酰胺基硫脲类化合物(Ⅱ1～Ⅱ8)。
2.
A novel compound——N-naphthalene acylN′-substituted p-chlorobenzamido thiocarbamide was synthesized by reaction of p-chlorobenzamido hydrazine and α-naphthalene acyl mustard oil,which was obtained by potassium thiocyanate combined with α-naphthalene acyl chloride formed from α-naphthylacetic acid and SOCl2 in anhydrous benzene.
通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯,然后与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯,再与对氯苯甲酰肼进行加成反应,合成了新型化合物N-萘乙酰基-N′-对氯苯甲酰氨基硫脲,用薄层色谱法跟踪最后一步反应,确定了反应时间。
3) 1'-Acetonaphthone
1-乙酰基萘
4) Acetylnaphthalene
α-乙酰基萘
5) β-acetylnaphthalene
β-乙酰基萘
6) acetonaphthol
乙酰基萘酚
补充资料：6-乙酰基-2-萘酚
分子式：C12H10O2
分子量：186.21
CAS号：10441-41-5
性质：棱状结晶（苯）。熔点171℃。置碱液中成黄色溶液。
制备方法：可用β-萘酚制取。
用途：萘普生的中间体。
分子量：186.21
CAS号：10441-41-5
性质：棱状结晶（苯）。熔点171℃。置碱液中成黄色溶液。
制备方法：可用β-萘酚制取。
用途：萘普生的中间体。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条