1) 2,6-hexanitrodiphenyl-amine-3,5-dinitropyridine
2,6-二苦氨基-3,5-二硝基吡啶
1.
The thermal decomposition process of 2,6-hexanitrodiphenyl-amine-3,5-dinitropyridine(PYX) was investigated by TG/DTG,TG/FTIR,TG/MS and therolysis rapid scan FTIR coupling techniques.
用热重-微商热重分析(TG/DTG)、热重与傅里叶变换红外联用技术(TG/FITR)、热重与质谱联用(TG/MS)和热裂解快速扫描傅里叶变换红外技术(RSC/FTIR)研究了PYX(2,6-二苦氨基-3,5-二硝基吡啶)热分解过程。
2) 2,6-diamino-3,5-dinitropyridine
2,6-二氨基-3,5-二硝基吡啶
1.
Preparation and Characterization of 2,6-Diamino-3,5-dinitropyridine (DADNP)
2,6-二氨基-3,5-二硝基吡啶的制备及表征
3) TYX
2,6-(双苦氨基)-3,5-硝基吡啶
4) 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO)
2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)
1.
In order to study the properties of 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO),the three refined samples of ANPyO were prepared by recrystallization from the solvents of trifluoroacetic acid(CF3COOH),dimethyl sulfoxide(DMSO) and N,N-dimethyl formamide(DMF) respectively,and the properties of the three samples were compared.
为了研究不同溶剂精制的2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)的性能,分别以三氟乙酸(CF3COOH)、二甲基亚砜(DMSO)和N,N-二甲基甲酰胺(DMF)为溶剂,采用重结晶法精制ANPyO,对精制后样品性能进行比较研究。
2.
2,6-Diamino-3,5-dinitropyridine(ANPy) and 2,6-diamino-3,5-dinitropyridine-1-oxide(ANPyO) was reacted with aqueous ammonia and KMnO4 under different conditions.
以氨水为胺化剂,KMnO4为氧化剂,在不同反应条件下实现2,6-二氨基-3,5-二硝基吡啶(ANPy)和2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)4位的氧化胺化反应,目标化合物2,4,6-三氨基-3,5-二硝基吡啶(TANPy)和2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物(TANPyO)的收率分别达到81。
5) 2,6-diamino-3,5-dinitropyridine-1-oxide
2,6-二氨基-3,5-二硝基吡啶-1-氧化物
1.
A novel synthetic method of 2,6-diamino-3,5-dinitropyridine-1-oxide (ANPyO) was explored using 2,6-diaminopyridine as the starting materials in three steps, including acetylation, N-oxidation and ni- tration.
研究了2,6-二氨基-3,5-二硝基吡啶-1-氧化物(ANPyO)的合成新方法。
2.
The results show that the best conditions are:DMSO as solvent and bubbling NH3 into the solution,the yield of the 2,4,6-triamino-3,5-dinitropyridine-1-oxide was up to 80%,and the content of 2,6-diamino-3,5-dinitropyridine-1-oxide was decrease to 0.
结果表明,以DMSO为溶剂、反应过程中不断通入氨气,胺化反应的收率和选择性最佳,2,4,6-三氨基-3,5-二硝基吡啶-1-氧化物的收率可达到80%,副产物2,6-二氨基-3,5-二硝基吡啶-1-氧化物的收率降低至0。
3.
A simple synthetic method of 2,6-diamino-3,5-dinitropyridine-1-oxide(DADNP-1-O) was de-scribed.
研究了2,6-二氨基-3,5-二硝基吡啶-1-氧化物(DADNP-1-O)的一个简易合成方法。
6) 2,6-diamino-3,5-dinitropyridine(ANPy)
2,6-二氨基-3,5-二硝基吡啶(ANPy)
补充资料：琰魔王苦乐二相
【琰魔王苦乐二相】
（传说）阎罗王宫昼夜三时有大铜镬，自然现出。时有大狱卒，捉王使卧热铁上。以铁钩开口，以洋铜灌之，全身无不燋烂。受此苦已，复与诸众生相娱乐，与诸大臣眷属同受福乐。见长阿含经十九地狱品，三界义。
（传说）阎罗王宫昼夜三时有大铜镬，自然现出。时有大狱卒，捉王使卧热铁上。以铁钩开口，以洋铜灌之，全身无不燋烂。受此苦已，复与诸众生相娱乐，与诸大臣眷属同受福乐。见长阿含经十九地狱品，三界义。
说明：补充资料仅用于学习参考，请勿用于其它任何用途。
参考词条